Search results for "Alkyl Compounds"

showing 3 items of 3 documents

Metodes izstrāde per- un polifluoralkil savienojumu noteikšanai pārtikas produktos, izmantojot augstas izšķirtspējas masspektrometriju

2022

Metodes izstrāde per- un polifluoralkil savienojumu noteikšanai pārtikas produktos, izmantojot augstas izšķirtspējas masspektrometriju. Jevņeviča K., zinātniskā vadītāja Mg.chem. Pasečnaja E. Bakalaura darbs, 41 lappuse, 5 attēli, 9 tabulas, 53 literatūras avoti. Latviešu valodā. Bakalaura darba ietvaros ir apkopota informācija par per- un polifluoralkil savienojumiem, to īpašībām, iedarbību uz cilvēkiem un apkārtējo vidi, toksicitāti, izplatību pārtikas produktos, kā arī ir apskatītas šo savienojumu noteikšanas metodes. Eksperimentālajā daļā ir izstrādāta un validēta analītiskā metode per- un polifluoralkil savienojumu noteikšanai pārtikas produktos, izmantojot augstas izšķirtspējas masspe…

HIGH RESOLUTION MASS SPECTROMETRYPER- UN POLIFLUORALKIL SAVIENOJUMIPER- AND POLIFLUORALKYL COMPOUNDSAUGSTAS IZŠĶIRTSPĒJAS MASSPEKTROMETRIJAPĀRTIKAS PRODUKTU PIESĀRŅOJUMSĶīmija
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Theoretical study of the effect of substituent and backbone conformation on the electronic properties of symmetrically substituted poly(di‐n‐alkylsil…

1994

We present the results of ab initio 3‐21G∗ geometry optimizations and valence effective Hamiltonian (VEH) band structure calculations aimed at determining the evolution of the geometric and electronic (ionization potential, electron affinities, and band gaps) properties of all‐trans poly(dimethylsilane), poly(diethylsilane), poly(di‐n‐propylsilane), and poly(di‐n‐butylsilane) when increasing the size of the alkyl group. In the latter polymer, we have also studied the 7/3 conformation, in order to analyze the effect of the backbone conformation on the geometric and electronic structure. The VEH ionization potentials of all‐trans poly(di‐n‐alkylsilanes) are almost equal, and as experimental p…

OptimizationEnergy GapPropyl CompoundsBand gapAb initioSubstituentGeometryGeneral Physics and AstronomyElectronic structurechemistry.chemical_compoundAb initio quantum chemistry methodsComputational chemistryMethyl CompoundsConformational ChangesPhysical and Theoretical ChemistryBand Structure:FÍSICA::Química física [UNESCO]Electronic band structureAlkyl Compounds ; Silanes ; Organic Polymers ; Conformational Changes ; Ab Initio Calculations ; Geometry ; Optimization ; Band Structure ; Affinity ; Ionization Potential ; Energy Gap ; Methyl Compounds ; Ethyl Compounds ; Propyl CompoundsDimethylsilaneOrganic PolymersSilanesUNESCO::FÍSICA::Química físicaCrystallographyAlkyl CompoundsIonization PotentialAffinitychemistryEthyl CompoundsIonization energyAb Initio Calculations
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Synthesis of polyfluoroalkyl sp2-iminosugar glycolipids and evaluation of their immunomodulatory properties towards anti-tumor, anti-leishmanial and …

2019

Immunomodulatory glycolipids, among which α-galactosylceramide (KRN7000) is an iconic example, have shown strong therapeutic potential in a variety of conditions ranging from cancer and infection to autoimmune or neurodegenerative diseases. A main difficulty for those channels is that they often provoke a cytokine storm comprising both pro- and anti-inflammatory mediators that antagonize each other and negatively affect the immune response. The synthesis of analogues with narrower cytokine secretion-inducing capabilities is hampered by the intrinsic difficulty at controlling the stereochemical outcome in glycosidation reactions, particularly if targeting the α-anomer, which seriously hamper…

Allosteric regulationIminosugar01 natural sciencesImmunomodulation03 medical and health sciencesGlycolipidGlycomimeticDrug DiscoverymedicineLeishmaniasisp38α MAPKCancer030304 developmental biologyInflammationPharmacology0303 health sciences010405 organic chemistryChemistryOrganic ChemistryAutophosphorylationBiological activityGeneral Medicinemedicine.disease0104 chemical sciencessp2-Iminosugar glycolipidsBiochemistryMechanism of actionPolyfluoroalkyl compoundsmedicine.symptomCytokine stormEuropean Journal of Medicinal Chemistry
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